Supplementary Material (ESI) for Chemical Communications.doc

SupplementaryMaterial(ESI)municationsThisjournalis©TheRoyalSocietyofChemistry2002DevelopmentofNewAcid-binatorialSynthesisonSolidSupportFrankStieberbandHerbertWaldmanna*a*AbteilungChemischeBiologie,Otto-Hahn-,44227Dortmund(Germany)andUniversitätDortmund,anischeChemie,44221Dortmund(Germany),Fax*49/231/133-2499,Phone*49/231/133-2400,E-mail:herbert.******@mpi-.-,SemaiaPharmaceuticalsGmbH&,Emil-Figge-Strasse76A44227Dortmund(Germany)ExperimentalSection GeneralProcedures::TheresinswerepurchasedfromRappPolymere,-functionalizedsupports6usingadipicaciddichloride(procedureA):Toasuspensionoftheappropiateamino-functionalizedresin3inCH2Cl2andpyridine(5:1,30ml/gresin)slowlyadipicaciddichloride(30eq.),theresinwashedwithTHF,THF/1 n HCl(1:1),THF,methanol,methylenechlorideundcyclohexane(2timeseach)-functionalizedsupports6usin