四丁基溴化铵结晶母液合成三丁胺的合成研究（毕业设计论文doc）.doc

学年论文
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四丁基溴化铵结晶母液合成三丁胺的合成研究
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专业
制药工程学
学生姓名

班级
B制药101
学号
1010309125
指导教师

完成日期
2013年06月05号
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四丁基溴化铵的合成研究
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摘要:主要说了四丁基溴化铵的合成,合成方法,以及合成后得到的残留的结晶母液的研究,用这个结晶母液制取溴化钙还有三丁胺,以达到废物利用的功效,产业多元化。
关键词:四丁基溴化铵;溴化钙;裂解;浓缩;结晶。
× Tetrabutylammonium bromide Synthesis of
Abstract: The tetrabutylammonium bromide said synthesis, synthesis method, and the resulting residue after the synthesis of the crystallization mother liquor of the study with the crystallization mother liquor from the system and tributylamine calcium bromide, to achieve the effect of the use of waste, industrial diversification.

目录
第一章文献综述···········································································1
四丁基溴化铵的物理化学性质···············································1
制备四丁基溴化铵的方法····················································1
·································································2
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本课题的意义··································································2
第二章实验部分············································································3
主要试剂及仪器··········································································3
从结晶母液中制备三丁胺和溴化钙的实验步骤·······················3
从实验中找出最佳催化剂的量···························4
第三章实验结果与讨论···························································
四丁基溴化铵结晶母液经一系列反应后所得产物量······
四丁基溴化铵在怎样温度下反应剧烈··························
实验结论···································································
致谢·······································································································4
第一章文献综述

  制备溴化钙的方法
四丁基溴化铵;Tetrabutyl ammonium bromide
其它名称:其它名称:TBAB、TBA溴化物、四正丁基氨基溴化物、溴化四丁铵, N,N,N-三丁基-1-丁铵溴化物
分子式:C16H36BrN
分子量:
CAS号:1643-19-2
熔点:103-104°C
性质:纯品为白色晶体或粉末,有潮解性,具有特殊气味,在常温、常压下稳定。溶于水、醇和丙酮,微溶于苯。水溶性600 g/L (20°C)。
用途:离子对试剂,用于巴氨西